Information card for entry 4337430

Structure parameters

• Formula: C39.5 H56.5 Cl N4 O2.5 Yb
• Calculated formula: C39.5 H56.5 Cl N4 O2.5 Yb
• Title of publication: Reversible Switching of Coordination Mode of ansa bis(Amidinate) Ligand in Ytterbium Complexes Driven by Oxidation State of the Metal Atom.
• Authors of publication: Tolpygin, Aleksei O.; Cherkasov, Anton V.; Fukin, Georgii K.; Trifonov, Alexander A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 3
• Pages of publication: 1537 - 1543
• a: 12.3731 ± 0.0007 Å
• b: 15.9925 ± 0.0009 Å
• c: 19.7268 ± 0.0011 Å
• α: 86.857 ± 0.001°
• β: 78.881 ± 0.001°
• γ: 82.954 ± 0.001°
• Cell volume: 3799.3 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0644
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0805
• Weighted residual factors for all reflections included in the refinement: 0.0873
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No