Information card for entry 4337542

Structure parameters

• Formula: C13 H16 Cl4 N2 O2 Pu
• Calculated formula: C13 H16 Cl4 N2 O2 Pu
• Title of publication: Supramolecular interactions in PuO2Cl4(2-) and PuCl6(2-) complexes with protonated pyridines: synthesis, crystal structures, and Raman spectroscopy.
• Authors of publication: Wilson, Richard E.; Schnaars, David D.; Andrews, Michael B.; Cahill, C. L.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 1
• Pages of publication: 383 - 392
• a: 12.6101 ± 0.0009 Å
• b: 11.6363 ± 0.0009 Å
• c: 12.2529 ± 0.0012 Å
• α: 90°
• β: 101.441 ± 0.001°
• γ: 90°
• Cell volume: 1762.2 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0246
• Residual factor for significantly intense reflections: 0.0179
• Weighted residual factors for significantly intense reflections: 0.0425
• Weighted residual factors for all reflections included in the refinement: 0.0458
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No