Information card for entry 4337567

Structure parameters

• Chemical name: acetonitrile(N"-(2,2'-bipyridinetricarbonyl-rhenium(I))-N,N'-diphenyl- isonicotinamidate)-tris(N,N'-diphenylisonicotinamidate)dirhodium(II,II) hexafluorophospate, acetonitrile 2.5 solvate
• Formula: C92 H74.5 F6 N17.5 O3 P Re Rh2
• Calculated formula: C92 H74.5 F6 N17.5 O3 P Re Rh2
• Title of publication: Rhodium amidinate dimers as structural and functional hubs for multimetallic assemblies.
• Authors of publication: Chartrand, Daniel; Hanan, Garry S.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 1
• Pages of publication: 624 - 636
• a: 12.692 ± 0.002 Å
• b: 17.182 ± 0.003 Å
• c: 21.751 ± 0.003 Å
• α: 75.315 ± 0.008°
• β: 77.197 ± 0.008°
• γ: 73.324 ± 0.007°
• Cell volume: 4338.3 ± 1.2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0775
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.1346
• Weighted residual factors for all reflections included in the refinement: 0.1422
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No