Information card for entry 4337835

Structure parameters

• Formula: C8 H7 Mo3 N3 O9
• Calculated formula: C8 H7 Mo3 N3 O9
• Title of publication: Synthesis, Structural Elucidation, and Catalytic Properties in Olefin Epoxidation of the Polymeric Hybrid Material [Mo3O9(2-[3(5)-Pyrazolyl]pyridine)]n.
• Authors of publication: Amarante, Tatiana R.; Neves, Patrícia; Gomes, Ana C.; Nolasco, Mariela M.; Ribeiro-Claro, Paulo; Coelho, Ana C.; Valente, Anabela A.; Paz, Filipe A Almeida; Smeets, Stef; McCusker, Lynne B.; Pillinger, Martyn; Gonçalves, Isabel S
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 5
• Pages of publication: 2652 - 2665
• a: 30.2491 ± 0.0005 Å
• b: 3.72717 ± 0.00005 Å
• c: 12.8518 ± 0.0003 Å
• α: 90°
• β: 110.196 ± 0.0016°
• γ: 90°
• Cell volume: 1359.88 ± 0.05 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 7.9
• Goodness-of-fit parameter for all reflections: 4.05
• Method of determination: powder diffraction
• Diffraction radiation wavelength: 0.826611 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No