Synthesis, Structural Characterization, Reactivity, and Catalytic Properties of Copper(I) Complexes with a Series of Tetradentate Tripodal Tris(pyrazolylmethyl)amine Ligands.
Authors of publication
Haldón, Estela; Delgado-Rebollo, Manuela; Prieto, Auxiliadora; Alvarez, Eleuterio; Maya, Celia; Nicasio, M. Carmen; Pérez, Pedro J
Journal of publication
Inorganic chemistry
Year of publication
2014
Journal volume
53
Journal issue
8
Pages of publication
4192 - 4201
a
17.8945 ± 0.0012 Å
b
12.0688 ± 0.0009 Å
c
19.1758 ± 0.0014 Å
α
90°
β
94.295 ± 0.002°
γ
90°
Cell volume
4129.7 ± 0.5 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
6
Space group number
13
Hermann-Mauguin space group symbol
P 1 2/c 1
Hall space group symbol
-P 2yc
Residual factor for all reflections
0.0857
Residual factor for significantly intense reflections
0.0679
Weighted residual factors for significantly intense reflections
0.1836
Weighted residual factors for all reflections included in the refinement
0.195
Goodness-of-fit parameter for all reflections included in the refinement
