Information card for entry 4338676

Structure parameters

• Formula: C129 H156 Si6
• Calculated formula: C129 H156 Si6
• Title of publication: Isolable 1,1-disubstituted silole dianion: a homogeneous two-electron-transfer reducing reagent.
• Authors of publication: Han, Zhengang; Li, Jianfeng; Hu, Hongfan; Zhang, Jianying; Cui, Chunming
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 12
• Pages of publication: 5890 - 5892
• a: 11.813 ± 0.002 Å
• b: 15.658 ± 0.003 Å
• c: 16.713 ± 0.003 Å
• α: 84.56 ± 0.03°
• β: 79.12 ± 0.03°
• γ: 81.76 ± 0.03°
• Cell volume: 2997.2 ± 1 ų
• Cell temperature: 113.15 K
• Ambient diffraction temperature: 113.15 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1437
• Residual factor for significantly intense reflections: 0.0789
• Weighted residual factors for significantly intense reflections: 0.1976
• Weighted residual factors for all reflections included in the refinement: 0.241
• Goodness-of-fit parameter for all reflections included in the refinement: 0.959
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No