Information card for entry 4340026

Structure parameters

• Formula: C32 H31 Ag B F4 N11
• Calculated formula: C32 H31 Ag B F4 N11
• Title of publication: Copper and Silver Complexes of Tris(triazole)amine and Tris(benzimidazole)amine Ligands: Evidence that Catalysis of an Azide-Alkyne Cycloaddition ("Click") Reaction by a Silver Tris(triazole)amine Complex Arises from Copper Impurities.
• Authors of publication: Connell, Timothy U.; Schieber, Christine; Silvestri, Ilaria Proietti; White, Jonathan M.; Williams, Spencer J.; Donnelly, Paul S.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 13
• Pages of publication: 6503 - 6511
• a: 11.8407 ± 0.0005 Å
• b: 12.2913 ± 0.0005 Å
• c: 14.6737 ± 0.0006 Å
• α: 108.487 ± 0.003°
• β: 96.896 ± 0.003°
• γ: 117.111 ± 0.004°
• Cell volume: 1712.01 ± 0.16 ų
• Cell temperature: 130 ± 0.2 K
• Ambient diffraction temperature: 130 ± 0.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0337
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.0841
• Weighted residual factors for all reflections included in the refinement: 0.087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No