Information card for entry 4340198

Structure parameters

• Formula: H44 K14 La2 O144 P4 W34
• Calculated formula: K11 La2 O144 P4 W34
• Title of publication: Production and reactions of organic-soluble lanthanide complexes of the monolacunary Dawson [alpha1-P2W17O61]10- polyoxotungstate.
• Authors of publication: Boglio, Cécile; Lenoble, Géraldine; Duhayon, Carine; Hasenknopf, Bernold; Thouvenot, René; Zhang, Cheng; Howell, Robertha C.; Burton-Pye, Benjamin P; Francesconi, Lynn C.; Lacôte, Emmanuel; Thorimbert, Serge; Malacria, Max; Afonso, Carlos; Tabet, Jean-Claude
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 3
• Pages of publication: 1389 - 1398
• a: 13.008 ± 0.002 Å
• b: 21.225 ± 0.004 Å
• c: 28.835 ± 0.006 Å
• α: 90°
• β: 92.857 ± 0.017°
• γ: 90°
• Cell volume: 7951 ± 3 ų
• Cell temperature: 295 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1721
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for all reflections: 0.1637
• Weighted residual factors for significantly intense reflections: 0.078
• Weighted residual factors for all reflections included in the refinement: 0.0779
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No