Information card for entry 4340249

Structure parameters

• Common name: W2(μ-hpp)2(η-hpp)2(μ-CO)2,2CH2Cl2
• Formula: C32 H52 Cl4 N12 O2 W2
• Calculated formula: C32 H52 Cl4 N12 O2 W2
• Title of publication: Facilitating access to the most easily ionized molecule: an improved synthesis of the key intermediate, W2(hpp)4Cl2, and related compounds.
• Authors of publication: Cotton, F. Albert; Donahue, James P.; Gruhn, Nadine E.; Lichtenberger, Dennis L.; Murillo, Carlos A.; Timmons, Daren J.; Van Dorn, Laura O.; Villagrán, Dino; Wang, Xiaoping
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 1
• Pages of publication: 201 - 213
• a: 9.1469 ± 0.0009 Å
• b: 10.8208 ± 0.001 Å
• c: 11.8963 ± 0.0012 Å
• α: 102.471 ± 0.002°
• β: 101.692 ± 0.002°
• γ: 114.904 ± 0.002°
• Cell volume: 983.81 ± 0.17 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0292
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0682
• Weighted residual factors for all reflections included in the refinement: 0.07
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No