Information card for entry 4340285

Structure parameters

• Formula: C21 H46 Cl N5 W
• Calculated formula: C21 H46 Cl N5 W
• SMILES: [W]1(Cl)([N](=C(N1C(C)C)N(C(C)C)C(C)C)C(C)C)(=NC(C)(C)C)=NC(C)(C)C
• Title of publication: Mixed guanidinato/alkylimido/azido tungsten(VI) complexes: synthesis and structural characterization.
• Authors of publication: Rische, Daniel; Baunemann, Arne; Winter, Manuela; Fischer, Roland A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 1
• Pages of publication: 269 - 277
• a: 9.059 ± 0.002 Å
• b: 10.359 ± 0.003 Å
• c: 15.293 ± 0.004 Å
• α: 81.786 ± 0.01°
• β: 80.206 ± 0.009°
• γ: 86.217 ± 0.007°
• Cell volume: 1398.4 ± 0.6 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.088
• Weighted residual factors for all reflections included in the refinement: 0.0917
• Goodness-of-fit parameter for all reflections included in the refinement: 0.821
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No