Information card for entry 4340572

Structure parameters

• Formula: C28 H41.74 B2 Cl0.26 Fe2 P2
• Calculated formula: C28 H41.741 B2 Cl0.259 Fe2 P2
• Title of publication: Cross-dehydrocoupling: A Novel Synthetic Route to P-B-P-B Chains.
• Authors of publication: Pandey, Souvik; Lönnecke, Peter; Hey-Hawkins, Evamarie
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 16
• Pages of publication: 8242 - 8249
• a: 10.0633 ± 0.0009 Å
• b: 10.7443 ± 0.0013 Å
• c: 13.2586 ± 0.0011 Å
• α: 88.886 ± 0.008°
• β: 85.612 ± 0.007°
• γ: 79.28 ± 0.009°
• Cell volume: 1404.4 ± 0.2 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1039
• Residual factor for significantly intense reflections: 0.0641
• Weighted residual factors for significantly intense reflections: 0.1408
• Weighted residual factors for all reflections included in the refinement: 0.1613
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No