Information card for entry 4340771

Structure parameters

• Formula: C45.5 H80 Fe K N2 O6 Si2
• Calculated formula: C45.5 H80 Fe K N2 O6 Si2
• Title of publication: Synthesis, structure, and magnetic and electrochemical properties of quasi-linear and linear iron(i), cobalt(i), and nickel(i) amido complexes.
• Authors of publication: Lin, Chun-Yi; Fettinger, James C.; Grandjean, Fernande; Long, Gary J.; Power, Philip P.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 17
• Pages of publication: 9400 - 9406
• a: 12.489 ± 0.003 Å
• b: 12.693 ± 0.003 Å
• c: 17.444 ± 0.004 Å
• α: 101.812 ± 0.003°
• β: 95.981 ± 0.003°
• γ: 104.259 ± 0.003°
• Cell volume: 2588.3 ± 1.1 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0781
• Weighted residual factors for all reflections included in the refinement: 0.0871
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No