Information card for entry 4340980

Structure parameters

• Common name: apx1292
• Formula: C38 H57 Cl2 N3 O2 U
• Calculated formula: C38 H57 Cl2 N3 O2 U
• SMILES: [U]1(Cl)([n]2c(c3[n]1ccc(c3)C(C)(C)C)cc(cc2)C(C)(C)C)(=Nc1c(cccc1C(C)C)C(C)C)(Cl)([O]1CCCC1)[O]1CCCC1
• Title of publication: Preparation and reactivity of the versatile uranium(IV) imido complexes U(NAr)Cl₂(R₂bpy)₂ (R = Me, (t)Bu) and U(NAr)Cl₂(tppo)₃.
• Authors of publication: Jilek, Robert E.; Tomson, Neil C.; Shook, Ryan L.; Scott, Brian L.; Boncella, James M.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 18
• Pages of publication: 9818 - 9826
• a: 10.8616 ± 0.0005 Å
• b: 11.6484 ± 0.0006 Å
• c: 15.7897 ± 0.0008 Å
• α: 99.832 ± 0.001°
• β: 91.493 ± 0.001°
• γ: 91.875 ± 0.001°
• Cell volume: 1966.31 ± 0.17 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.019
• Residual factor for significantly intense reflections: 0.0172
• Weighted residual factors for significantly intense reflections: 0.0432
• Weighted residual factors for all reflections included in the refinement: 0.0438
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No