Information card for entry 4341028

Structure parameters

• Formula: C22 H62 N3 O S3 Si6 Y
• Calculated formula: C22 H62 N3 O S3 Si6 Y
• Title of publication: Cocrystallization of (μ-S2)(2-) and (μ-S)(2-) and Formation of an [η(2)-S3N(SiMe3)2] Ligand from Chalcogen Reduction by (N2)(2-) in a Bimetallic Yttrium Amide Complex.
• Authors of publication: Corbey, Jordan F.; Fang, Ming; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 3
• Pages of publication: 801 - 807
• a: 8.8099 ± 0.0005 Å
• b: 10.0494 ± 0.0006 Å
• c: 23.8094 ± 0.0014 Å
• α: 101.062 ± 0.0008°
• β: 90.9696 ± 0.0008°
• γ: 101.795 ± 0.0008°
• Cell volume: 2021.6 ± 0.2 ų
• Cell temperature: 88 ± 2 K
• Ambient diffraction temperature: 88 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0513
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0753
• Weighted residual factors for all reflections included in the refinement: 0.0805
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No