Information card for entry 4341206

Structure parameters

• Formula: C15 H39 N4 Si3 V
• Calculated formula: C15 H39 N4 Si3 V
• Title of publication: Role of Axial Base Coordination in Isonitrile Binding and Chalcogen Atom Transfer to Vanadium(III) Complexes.
• Authors of publication: Majumdar, Subhojit; Stauber, Julia M.; Palluccio, Taryn D.; Cai, Xiaochen; Velian, Alexandra; Rybak-Akimova, Elena V; Temprado, Manuel; Captain, Burjor; Cummins, Christopher C.; Hoff, Carl D.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Pages of publication: 141003140335004
• a: 9.0256 ± 0.0009 Å
• b: 16.1071 ± 0.0015 Å
• c: 16.6515 ± 0.0016 Å
• α: 90°
• β: 93.029 ± 0.002°
• γ: 90°
• Cell volume: 2417.4 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0475
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1176
• Weighted residual factors for all reflections included in the refinement: 0.1221
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No