Information card for entry 4341574

Structure parameters

• Formula: C83 H73.15 Mg N2 O0.15
• Calculated formula: C83 H73.15 Mg N2 O0.15
• Title of publication: Mononuclear Three-Coordinate Magnesium Complexes of a Highly Sterically Encumbered β-Diketiminate Ligand.
• Authors of publication: Arrowsmith, Merle; Maitland, Brant; Kociok-Köhn, Gabriele; Stasch, Andreas; Jones, Cameron; Hill, Michael S.
• Journal of publication: Inorganic chemistry
• Year of publication: 2014
• Journal volume: 53
• Journal issue: 19
• Pages of publication: 10543 - 10552
• a: 13.1932 ± 0.0001 Å
• b: 13.2993 ± 0.0001 Å
• c: 36.9496 ± 0.0004 Å
• α: 87.7914 ± 0.0005°
• β: 88.9917 ± 0.0004°
• γ: 89.9024 ± 0.0005°
• Cell volume: 6477.37 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1074
• Residual factor for significantly intense reflections: 0.0666
• Weighted residual factors for significantly intense reflections: 0.1531
• Weighted residual factors for all reflections included in the refinement: 0.172
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No