Information card for entry 4341631

Structure parameters

• Formula: C7.2 H97.2 N3.6 Na12 O120 Sb2 W20.2 Zn1.8
• Calculated formula: C7.528 H5.646 N3.764 Na12 O120.064 Sb2 W20.118 Zn1.882
• Title of publication: Functionalization of krebs-type polyoxometalates with n,o-chelating ligands: a systematic study.
• Authors of publication: Artetxe, Beñat; Reinoso, Santiago; San Felices, Leire; Vitoria, Pablo; Pache, Aroa; Martín-Caballero, Jagoba; Gutiérrez-Zorrilla, Juan M
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 1
• Pages of publication: 241 - 252
• a: 13.845 ± 0.0004 Å
• b: 14.6579 ± 0.0004 Å
• c: 15.7431 ± 0.0004 Å
• α: 68.89 ± 0.002°
• β: 70.831 ± 0.002°
• γ: 87.242 ± 0.002°
• Cell volume: 2806.29 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.028
• Residual factor for significantly intense reflections: 0.0253
• Weighted residual factors for significantly intense reflections: 0.0555
• Weighted residual factors for all reflections included in the refinement: 0.0566
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No