Information card for entry 4343081

Structure parameters

• Formula: C41 H37 B4 Cl2 F12 N2 O6 Sb
• Calculated formula: C40 H37 B4 F12 N2 O6 Sb
• Title of publication: From Stiba- and Bismaheteroboroxines to N,C,N-Chelated Diorganoantimony(III) and Bismuth(III) Cations-An Unexpected Case of Aryl Group Migration.
• Authors of publication: Dostál, Libor; Jambor, Roman; Růžička, Aleš; Jirásko, Robert; Lyčka, Antonín; Beckmann, Jens; Ketkov, Sergey
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 12
• Pages of publication: 6010 - 6019
• a: 12.0481 ± 0.0007 Å
• b: 15.415 ± 0.001 Å
• c: 15.8549 ± 0.001 Å
• α: 63.29 ± 0.005°
• β: 71.087 ± 0.004°
• γ: 86.852 ± 0.004°
• Cell volume: 2474 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2384
• Residual factor for significantly intense reflections: 0.1188
• Weighted residual factors for significantly intense reflections: 0.2617
• Weighted residual factors for all reflections included in the refinement: 0.3413
• Goodness-of-fit parameter for all reflections included in the refinement: 1.427
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No