Crystallography Open Database

Information card for entry 4343300

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Coordinates	4343300.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C76 H65 B F24 N3 Rh
Calculated formula	C76 H65 B F24 N3 Rh
Title of publication	Synthesis and Reactivity toward H2 of (η(5)-C5Me5)Rh(III) Complexes with Bulky Aminopyridinate Ligands.
Authors of publication	Zamorano, Ana; Rendón, Nuria; Valpuesta, José E V; Álvarez, Eleuterio; Carmona, Ernesto
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	13
Pages of publication	6573 - 6581
a	13.1948 ± 0.0005 Å
b	15.2656 ± 0.0005 Å
c	18.6573 ± 0.0007 Å
α	91.247 ± 0.0009°
β	96.662 ± 0.001°
γ	102.135 ± 0.001°
Cell volume	3645.2 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0733
Residual factor for significantly intense reflections	0.0534
Weighted residual factors for significantly intense reflections	0.1371
Weighted residual factors for all reflections included in the refinement	0.1513
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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