Synthesis and Temperature-Induced Structural Phase and Spin Transitions in Hexadecylboron-Capped Cobalt(II) Hexachloroclathrochelate and Its Diamagnetic Iron(II)-Encapsulating Analogue.
Authors of publication
Vologzhanina, Anna V.; Belov, Alexander S.; Novikov, Valentin V.; Dolganov, Alexander V.; Romanenko, Galina V.; Ovcharenko, Victor I.; Korlyukov, Alexander A.; Buzin, Mikhail I.; Voloshin, Yan Z.
Journal of publication
Inorganic chemistry
Year of publication
2015
Journal volume
54
Journal issue
12
Pages of publication
5827 - 5838
a
45.321 ± 0.003 Å
b
7.966 ± 0.001 Å
c
14.003 ± 0.001 Å
α
90°
β
101.675 ± 0.005°
γ
90°
Cell volume
4950.9 ± 0.8 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
7
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.133
Residual factor for significantly intense reflections
0.044
Weighted residual factors for significantly intense reflections
0.0725
Weighted residual factors for all reflections included in the refinement
0.0856
Goodness-of-fit parameter for all reflections included in the refinement
