Information card for entry 4344031

Structure parameters

• Formula: C87 H118 N6 O24 Tm4
• Calculated formula: C87 H108 N6 O24 Tm4
• Title of publication: Tetranuclear and Pentanuclear Compounds of the Rare-Earth Metals: Synthesis and Magnetism.
• Authors of publication: Yadav, Munendra; Mondal, Abhishake; Mereacre, Valeriu; Jana, Salil Kumar; Powell, Annie K.; Roesky, Peter W.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 16
• Pages of publication: 7846 - 7856
• a: 13.9186 ± 0.0005 Å
• b: 17.6449 ± 0.0005 Å
• c: 21.6536 ± 0.0008 Å
• α: 68.463 ± 0.002°
• β: 85.537 ± 0.003°
• γ: 72.381 ± 0.002°
• Cell volume: 4711.3 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for significantly intense reflections: 0.0866
• Weighted residual factors for all reflections included in the refinement: 0.0903
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No