Information card for entry 4344379

Structure parameters

• Common name: 2014-05-12
• Formula: H148 Li12 Na8 Ni2 O186 P4 W30
• Calculated formula: Li8 Na5.9998 Ni2 O169 P4 W30.0062
• Title of publication: Syntheses, Structural Characterization, and Catalytic Properties of Di- and Trinickel Polyoxometalates.
• Authors of publication: Guo, Weiwei; Lv, Hongjin; Bacsa, John; Gao, Yuanzhe; Lee, Je Seong; Hill, Craig L.
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 2
• Pages of publication: 461 - 466
• a: 13.2155 ± 0.0015 Å
• b: 13.38 ± 0.002 Å
• c: 25.206 ± 0.004 Å
• α: 75.983 ± 0.002°
• β: 81.838 ± 0.002°
• γ: 61.811 ± 0.001°
• Cell volume: 3809.4 ± 0.9 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0775
• Residual factor for significantly intense reflections: 0.0509
• Weighted residual factors for significantly intense reflections: 0.1148
• Weighted residual factors for all reflections included in the refinement: 0.1273
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No