Information card for entry 4344594

Structure parameters

• Formula: C69 H90 Cl6 F12 N8 Ni2 Sb2
• Calculated formula: C69 H90 Cl6 F12 N8 Ni2 Sb2
• Title of publication: Geometric and Electronic Structures of Nickel(II) Complexes of Redox Noninnocent Tetradentate Phenylenediamine Ligands.
• Authors of publication: Ciccione, Jérémie; Leconte, Nicolas; Luneau, Dominique; Philouze, Christian; Thomas, Fabrice
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 2
• Pages of publication: 649 - 665
• a: 9.4927 ± 0.0019 Å
• b: 12.896 ± 0.003 Å
• c: 16.95 ± 0.003 Å
• α: 80.96 ± 0.03°
• β: 87.72 ± 0.03°
• γ: 71.86 ± 0.03°
• Cell volume: 1947.3 ± 0.8 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0593
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.0817
• Weighted residual factors for all reflections included in the refinement: 0.0907
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No