Information card for entry 4344785

Structure parameters

• Formula: C56 H43 B F24 N4 O2 Rh
• Calculated formula: C56 H43 B F24 N4 O2 Rh
• Title of publication: Reexamining Oxidation States during the Synthesis of 2-Rhodaoxetanes from Olefins.
• Authors of publication: Desnoyer, Addison N.; Behyan, Shirin; Patrick, Brian O.; Dauth, Alexander; Love, Jennifer A.; Kennepohl, Pierre
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 55
• Journal issue: 1
• Pages of publication: 13
• a: 9.7614 ± 0.0011 Å
• b: 17.681 ± 0.002 Å
• c: 18.517 ± 0.002 Å
• α: 65.05 ± 0.006°
• β: 85.142 ± 0.006°
• γ: 75.089 ± 0.006°
• Cell volume: 2799 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1052
• Residual factor for significantly intense reflections: 0.0708
• Weighted residual factors for significantly intense reflections: 0.1414
• Weighted residual factors for all reflections included in the refinement: 0.1513
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No