Information card for entry 4344931

Structure parameters

• Formula: C52 H74 F6 N4 O6 Sb U
• Calculated formula: C52 H74 F6 N4 O6 Sb U
• Title of publication: Uranium Tetrakis-Aryloxide Derivatives Supported by Tetraazacyclododecane: Synthesis of Air-Stable, Coordinatively-Unsaturated U(IV) and U(V) Complexes.
• Authors of publication: Hümmer, Julian; Heinemann, Frank W.; Meyer, Karsten
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• Journal volume: 56
• Journal issue: 6
• Pages of publication: 3201 - 3206
• a: 12.5028 ± 0.0013 Å
• b: 13.249 ± 0.0015 Å
• c: 17.1043 ± 0.0019 Å
• α: 102.392 ± 0.002°
• β: 99.172 ± 0.002°
• γ: 92.988 ± 0.002°
• Cell volume: 2721 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0341
• Residual factor for significantly intense reflections: 0.0273
• Weighted residual factors for significantly intense reflections: 0.0595
• Weighted residual factors for all reflections included in the refinement: 0.0621
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No