Information card for entry 4345541

Structure parameters

• Formula: C66 H66 B4 Co2 N18 O2
• Calculated formula: C66 H66 B4 Co2 N18 O2
• Title of publication: Reactions of Neutral Cobalt(II) Complexes of a Dianionic Tetrapodal Pentadentate Ligand: Cobalt(III) Amides from Imido Radicals.
• Authors of publication: Nurdin, Lucie; Spasyuk, Denis M.; Piers, Warren E.; Maron, Laurent
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• a: 13.9846 ± 0.0014 Å
• b: 22.079 ± 0.002 Å
• c: 19.893 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6142.3 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0552
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.1098
• Weighted residual factors for all reflections included in the refinement: 0.1178
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No