Information card for entry 4345665

Structure parameters

• Chemical name: 1-tert-Butanolato-(2,8,9-trioxa-5-aza-3,3,6,6-tetramethyl-1- germatricyclo[3.3.3.01,5]undecane
• Formula: C31 H58 Ge2 N2 O8
• Calculated formula: C31 H58 Ge2 N2 O8
• Title of publication: Introducing Stereogenic Centers to Group XIV Metallatranes.
• Authors of publication: Glowacki, Britta; Lutter, Michael; Alnasr, Hazem; Seymen, Rana; Hiller, Wolf; Jurkschat, Klaus
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• a: 14.2668 ± 0.0006 Å
• b: 13.2833 ± 0.0005 Å
• c: 18.8304 ± 0.0012 Å
• α: 90°
• β: 95.253 ± 0.005°
• γ: 90°
• Cell volume: 3553.6 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1237
• Residual factor for significantly intense reflections: 0.0914
• Weighted residual factors for significantly intense reflections: 0.2339
• Weighted residual factors for all reflections included in the refinement: 0.24
• Goodness-of-fit parameter for all reflections included in the refinement: 1.971
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No