Information card for entry 4345670

Structure parameters

• Formula: C72 H212 O3 Si28 Yb2
• Calculated formula: C72 H212 O3 Si28 Yb2
• Title of publication: Using Functionalized Silyl Ligands To Suppress Solvent Coordination to Silyl Lanthanide(II) Complexes.
• Authors of publication: Zitz, Rainer; Hlina, Johann; Aghazadeh Meshgi, Mohammad; Krenn, Heinz; Marschner, Christoph; Szilvási, Tibor; Baumgartner, Judith
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• a: 19.344 ± 0.004 Å
• b: 20.358 ± 0.004 Å
• c: 36.442 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14351 ± 5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1298
• Residual factor for significantly intense reflections: 0.0987
• Weighted residual factors for significantly intense reflections: 0.262
• Weighted residual factors for all reflections included in the refinement: 0.2835
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No