Information card for entry 4346052

Structure parameters

• Formula: C6 H96 Ga11.8 In1.2 N15 O99
• Calculated formula: Ga11.86 In1.14 N12 O84
• Title of publication: Synthesis and solid-state structural characterization of a series of aqueous heterometallic tridecameric group 13 clusters.
• Authors of publication: Kamunde-Devonish, Maisha K; Fast, Dylan B.; Mensinger, Zachary L.; Gatlin, Jason T.; Zakharov, Lev N.; Dolgos, Michelle R.; Johnson, Darren W.
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 8
• Pages of publication: 3913 - 3920
• a: 20.1387 ± 0.0014 Å
• b: 20.1387 ± 0.0014 Å
• c: 18.49 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 6494.3 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0391
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0886
• Weighted residual factors for all reflections included in the refinement: 0.0916
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No