Sodium thioether macrocyclic chemistry: remarkable homoleptic octathia coordination to Na(+).
Authors of publication
Champion, Martin J. D.; Dyke, John M.; Levason, William; Light, Mark E.; Pugh, David; Bhakhoa, Hanusha; Rhyman, Lydia; Ramasami, Ponnadurai; Reid, Gillian
Journal of publication
Inorganic chemistry
Year of publication
2015
Journal volume
54
Journal issue
6
Pages of publication
2497 - 2499
a
12.8461 ± 0.0016 Å
b
12.9256 ± 0.0017 Å
c
18.696 ± 0.002 Å
α
80.074 ± 0.005°
β
72.78 ± 0.004°
γ
89.917 ± 0.006°
Cell volume
2916.8 ± 0.6 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0989
Residual factor for significantly intense reflections
0.0847
Weighted residual factors for significantly intense reflections
0.2255
Weighted residual factors for all reflections included in the refinement
0.2316
Goodness-of-fit parameter for all reflections included in the refinement
