Information card for entry 4346238

Structure parameters

• Formula: C36 H44 F24 Ni4 O14 P4
• Calculated formula: C36 H44 F24 Ni4 O14 P4
• Title of publication: Transition Metal Complexes of Phosphinous Acids Featuring a Quasichelating Unit: Synthesis, Characterization, and Hetero-bimetallic Complexes.
• Authors of publication: Allefeld, Nadine; Bader, Julia; Neumann, Beate; Stammler, Hans-Georg; Ignat'ev, Nikolai; Hoge, Berthold
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 16
• Pages of publication: 7945 - 7952
• a: 9.1196 ± 0.0006 Å
• b: 9.4568 ± 0.0006 Å
• c: 17.0109 ± 0.0011 Å
• α: 100.628 ± 0.002°
• β: 103.287 ± 0.002°
• γ: 100.273 ± 0.002°
• Cell volume: 1365.42 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.046
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.1218
• Weighted residual factors for all reflections included in the refinement: 0.1241
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No