Information card for entry 4346638

Structure parameters

• Formula: C120 H168 Cu9 N72 O0 W6
• Calculated formula: C120 H168 Cu9 N72 W6
• Title of publication: Electrochemical Synthesis and Magnetic Properties of [Cu9W6]: The Ultimate Member of the Quindecanuclear Octacyanometallate-Based Transition-Metal Cluster?
• Authors of publication: Zhang, Zaichao; Liu, Yong; Wei, Rong-Min; Sheng, Zhen-Huan; Wang, Peng; Song, You
• Journal of publication: Inorganic chemistry
• Year of publication: 2015
• Journal volume: 54
• Journal issue: 23
• Pages of publication: 11049 - 11051
• a: 17.796 ± 0.003 Å
• b: 17.665 ± 0.003 Å
• c: 28.23 ± 0.004 Å
• α: 90°
• β: 91.778 ± 0.002°
• γ: 90°
• Cell volume: 8870 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.1107
• Weighted residual factors for all reflections included in the refinement: 0.1196
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No