Information card for entry 4346876

Structure parameters

• Formula: C44 H32 Cl4 N P Pt
• Calculated formula: C44 H32 Cl4 N P Pt
• SMILES: C(Cl)Cl.[Pt]([P](c1ccccc1)(c1ccccc1)c1ccccc1)(Cl)(Cl)[n]1c2ccc3ccc4ccc5ccc6ccccc6c5c4c3c2ccc1
• Title of publication: Synthesis and Structural Properties of Aza[n]helicene Platinum Complexes: Control of Cis and Trans Stereochemistry.
• Authors of publication: Mendola, Daniele; Saleh, Nidal; Hellou, Nora; Vanthuyne, Nicolas; Roussel, Christian; Toupet, Loïc; Castiglione, Franca; Melone, Federica; Caronna, Tullio; Fontana, Francesca; Martí-Rujas, Javier; Parisini, Emilio; Malpezzi, Luciana; Mele, Andrea; Crassous, Jeanne
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 5
• Pages of publication: 2009 - 2017
• a: 10.6352 ± 0.0005 Å
• b: 14.665 ± 0.0009 Å
• c: 14.7018 ± 0.0008 Å
• α: 61.388 ± 0.006°
• β: 69.548 ± 0.005°
• γ: 79.328 ± 0.005°
• Cell volume: 1885.6 ± 0.2 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0814
• Residual factor for significantly intense reflections: 0.0617
• Weighted residual factors for significantly intense reflections: 0.1498
• Weighted residual factors for all reflections included in the refinement: 0.1589
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No