Information card for entry 4346914

Structure parameters

• Formula: C122 Cl12 Cu4 F24 Fe Gd2 N6 O78 Si2 W18
• Calculated formula: C122 Cl12 Cu4 F24 Fe Gd2 N6 O78 Si2 W18
• Title of publication: Sequential Synthesis of 3d-3d'-4f Heterometallic Heptanuclear Clusters in between Lacunary Polyoxometalates.
• Authors of publication: Sato, Rinta; Suzuki, Kosuke; Minato, Takuo; Yamaguchi, Kazuya; Mizuno, Noritaka
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 5
• Pages of publication: 2023 - 2029
• a: 19.6894 ± 0.0002 Å
• b: 20.1629 ± 0.0002 Å
• c: 26.5399 ± 0.0003 Å
• α: 90°
• β: 100.56°
• γ: 90°
• Cell volume: 10357.8 ± 0.19 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 10
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0641
• Residual factor for significantly intense reflections: 0.0556
• Weighted residual factors for significantly intense reflections: 0.1588
• Weighted residual factors for all reflections included in the refinement: 0.1688
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No