Information card for entry 4347219

Structure parameters

• Formula: C20 H18 F7 N4 O2 Sb V
• Calculated formula: C20 H18 F7 N4 O2 Sb V
• SMILES: [Sb](F)(F)(F)(F)(F)[F-].[V]12(F)([n]3c(c4[n]1cccc4)cccc3)([n]1c(c3[n]2cccc3)cccc1)=O.O
• Title of publication: Synthesis, Bonding, and Reactivity of Vanadium(IV) Oxido-Fluorido Compounds with Neutral Chelate Ligands of the General Formula cis-[V(IV)(═O)(F)(L(N-N))2](+).
• Authors of publication: Passadis, Stamatis S.; Tsiafoulis, Constantinos; Drouza, Chryssoula; Tsipis, Athanassios C.; Miras, Haralampos N.; Keramidas, Anastasios D.; Kabanos, Themistoklis A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 4
• Pages of publication: 1364 - 1366
• a: 8.1049 ± 0.0003 Å
• b: 10.4872 ± 0.0004 Å
• c: 13.8978 ± 0.0006 Å
• α: 84.346 ± 0.003°
• β: 75.05 ± 0.004°
• γ: 89.048 ± 0.003°
• Cell volume: 1135.7 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0495
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.0857
• Weighted residual factors for all reflections included in the refinement: 0.0938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No