Information card for entry 4347481

Structure parameters

• Formula: C48 H52 As Cl N P
• Calculated formula: C48.0048 H52.0052 As1.0001 Cl1.0001 N1.0001 P1.0001
• Title of publication: Synthesis of Heavy Cyclodipnictadiphosphanes [ClE(μ-P-Ter)]2 [E = P, As, Sb, or Bi; Ter = 2,6-bis(2,4,6-trimethylphenyl)phenyl].
• Authors of publication: Hinz, Alexander; Schulz, Axel; Villinger, Alexander
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 7
• Pages of publication: 3692 - 3699
• a: 15.9653 ± 0.0005 Å
• b: 14.5149 ± 0.0005 Å
• c: 17.7782 ± 0.0006 Å
• α: 90°
• β: 91.854 ± 0.001°
• γ: 90°
• Cell volume: 4117.7 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0732
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1014
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No