Crystallography Open Database

Information card for entry 4347832

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Coordinates	4347832.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C59 H73 B N2 O6 P2 Ru
Calculated formula	C59 H73 B N2 O6 P2 Ru
Title of publication	Pentamethylcyclopentadienyl Half-Sandwich Diazoalkane Complexes of Ruthenium: Preparation and Reactivity.
Authors of publication	Albertin, Gabriele; Antoniutti, Stefano; Bortoluzzi, Marco; Botter, Alessandra; Castro, Jesús
Journal of publication	Inorganic chemistry
Year of publication	2016
Journal volume	55
Journal issue	11
Pages of publication	5592 - 5602
a	13.7683 ± 0.001 Å
b	21.0912 ± 0.0018 Å
c	19.7024 ± 0.0014 Å
α	90°
β	94.161 ± 0.003°
γ	90°
Cell volume	5706.3 ± 0.8 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0693
Residual factor for significantly intense reflections	0.0484
Weighted residual factors for significantly intense reflections	0.1267
Weighted residual factors for all reflections included in the refinement	0.1423
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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