Information card for entry 4348041

Structure parameters

• Common name: jaa18_0m
• Chemical name: K2[(C13H9NO8)Ni(H2O)] 2(H2O)
• Formula: C13 H15 K2 N Ni O11
• Calculated formula: C13 H11 K2 N Ni O11
• Title of publication: Synthesis and Characterization of a Tetrapodal NO4(4-) Ligand and Its Transition Metal Complexes.
• Authors of publication: Axelson, Jordan C.; Gonzalez, Miguel I.; Meihaus, Katie R.; Chang, Christopher J.; Long, Jeffrey R.
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 15
• Pages of publication: 7527 - 7534
• a: 7.58 ± 0.0002 Å
• b: 10.34 ± 0.0003 Å
• c: 10.759 ± 0.0003 Å
• α: 82.241 ± 0.001°
• β: 88.369 ± 0.001°
• γ: 87.154 ± 0.001°
• Cell volume: 834.31 ± 0.04 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for significantly intense reflections: 0.0745
• Weighted residual factors for all reflections included in the refinement: 0.0754
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No