Information card for entry 4348050

Structure parameters

• Formula: C22 H20 As1.83 Fe4 N O14 P1.17
• Calculated formula: C22 H20 As1.827 Fe4 N O14 P1.173
• Title of publication: New Main-Group-Element-Rich nido-Octahedral Cluster System: Synthesis and Characterization of [Et4N][Fe2(CO)6(μ3-As){μ3-EFe(CO)4}2].
• Authors of publication: Schipper, Desmond E.; Ikhlef, Djamila; Khalal, Samila; Saillard, Jean-Yves; Whitmire, Kenton H.
• Journal of publication: Inorganic chemistry
• Year of publication: 2016
• Journal volume: 55
• Journal issue: 13
• Pages of publication: 6679 - 6684
• a: 9.736 ± 0.003 Å
• b: 13.57 ± 0.004 Å
• c: 13.803 ± 0.005 Å
• α: 68.272 ± 0.011°
• β: 81.975 ± 0.012°
• γ: 75.414 ± 0.013°
• Cell volume: 1637.3 ± 0.9 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for significantly intense reflections: 0.09
• Weighted residual factors for all reflections included in the refinement: 0.1133
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No