Information card for entry 4349363

Structure parameters

• Formula: C33 H55 B Cl F4 N O2 Os P2
• Calculated formula: C33 H55 B Cl F4 N O2 Os P2
• Title of publication: mer, fac, and Bidentate Coordination of an Alkyl-POP Ligand in the Chemistry of Nonclassical Osmium Hydrides.
• Authors of publication: Esteruelas, Miguel A.; García-Yebra, Cristina; Martín, Jaime; Oñate, Enrique
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• Journal volume: 56
• Journal issue: 1
• Pages of publication: 676 - 683
• a: 11.843 ± 0.003 Å
• b: 22.139 ± 0.005 Å
• c: 14.179 ± 0.003 Å
• α: 90°
• β: 89.988 ± 0.003°
• γ: 90°
• Cell volume: 3717.6 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.082
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1143
• Weighted residual factors for all reflections included in the refinement: 0.1289
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No