Information card for entry 4349380

Structure parameters

• Formula: C22 H51 Al Co N2 Si4
• Calculated formula: C22 H51 Al Co N2 Si4
• Title of publication: Diverse Reactivity of ECp* (E = Al, Ga) toward Low-Coordinate Transition Metal Amides [TM(N(SiMe₃)₂)₂] (TM = Fe, Co, Zn): Insertion, Cp* Transfer, and Orthometalation.
• Authors of publication: Weßing, Jana; Göbel, Christoph; Weber, Birgit; Gemel, Christian; Fischer, Roland A.
• Journal of publication: Inorganic chemistry
• Year of publication: 2017
• Journal volume: 56
• Journal issue: 6
• Pages of publication: 3517 - 3525
• a: 12.4018 ± 0.0002 Å
• b: 18.465 ± 0.0003 Å
• c: 14.0269 ± 0.0002 Å
• α: 90°
• β: 104.914 ± 0.002°
• γ: 90°
• Cell volume: 3103.94 ± 0.09 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0433
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for significantly intense reflections: 0.0865
• Weighted residual factors for all reflections included in the refinement: 0.0902
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No