Information card for entry 4350212

Structure parameters

• Formula: C44 H44 N4 Ni2 O4
• Calculated formula: C44 H44 N4 Ni2 O4
• Title of publication: Dinuclear nickel and palladium complexes with bridging 2,5-diamino-1,4-benzoquinonediimines: synthesis, structures, and catalytic oligomerization of ethylene.
• Authors of publication: Taquet, Jean-Philippe; Siri, Olivier; Braunstein, Pierre; Welter, Richard
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 12
• Pages of publication: 4668 - 4676
• a: 8.348 ± 0.001 Å
• b: 11.403 ± 0.002 Å
• c: 11.905 ± 0.002 Å
• α: 95.18 ± 0.05°
• β: 110.25 ± 0.05°
• γ: 111.35 ± 0.05°
• Cell volume: 959.4 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1101
• Residual factor for significantly intense reflections: 0.0644
• Weighted residual factors for significantly intense reflections: 0.1123
• Weighted residual factors for all reflections included in the refinement: 0.1263
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No