Information card for entry 4350334

Structure parameters

• Formula: H51 K15 O147 P4 W34 Zr
• Calculated formula: K15 O147 P4 W34 Zr
• Title of publication: Syntheses and X-ray crystal structures of zirconium(IV) and hafnium(IV) complexes containing monovacant wells-Dawson and Keggin polyoxotungstates.
• Authors of publication: Kato, Chika Nozaki; Shinohara, Akira; Hayashi, Kunihiko; Nomiya, Kenji
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 20
• Pages of publication: 8108 - 8119
• a: 47.374 ± 0.005 Å
• b: 14.4975 ± 0.0015 Å
• c: 22.739 ± 0.002 Å
• α: 90°
• β: 91.141 ± 0.001°
• γ: 90°
• Cell volume: 15614 ± 3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0509
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1281
• Weighted residual factors for all reflections included in the refinement: 0.133
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No