Information card for entry 4350385

Structure parameters

• Common name: Complex 9 (Tekeste), [(Tp(Ph,Me)Zn)2]-OH-tetraphenylborat
• Chemical name: Bis[Hydrotris(3-phenyl-5-methyl-pyrazol-1-yl)borato-zink]-Hydroxid-ph4B
• Formula: C90 H88 B3 N12 O3 Zn2
• Calculated formula: C90 H88 B3 N12 O3 Zn2
• Title of publication: Zn-OH2 and Zn-OH complexes with hydroborate-derived tripod ligands: a comprehensive study.
• Authors of publication: Ibrahim, Mohamed M.; Olmo, Cristina Pérez; Tekeste, Teame; Seebacher, Jan; He, Guosen; Maldonado Calvo, José A; Böhmerle, Karin; Steinfeld, Gunther; Brombacher, Horst; Vahrenkamp, Heinrich
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 18
• Pages of publication: 7493 - 7502
• a: 24.576 ± 0.004 Å
• b: 14.463 ± 0.002 Å
• c: 22.823 ± 0.004 Å
• α: 90°
• β: 100.554 ± 0.003°
• γ: 90°
• Cell volume: 7975 ± 2 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.0933
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.1105
• Weighted residual factors for all reflections included in the refinement: 0.136
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No