Information card for entry 4350624

Structure parameters

• Formula: C40 H69 Li2 N4 O2 Sb
• Calculated formula: C40 H69 Li2 N4 O2 Sb
• Title of publication: Bis(1 degree-amino)cyclodistib(III)azanes: the first structural characterization of cis and trans isomers of a single cyclodipnict(III)azane.
• Authors of publication: Eisler, Dana J.; Chivers, Tristram
• Journal of publication: Inorganic chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 26
• Pages of publication: 10734 - 10742
• a: 10.705 ± 0.002 Å
• b: 20.816 ± 0.004 Å
• c: 20.97 ± 0.004 Å
• α: 107.63 ± 0.03°
• β: 92.5 ± 0.03°
• γ: 91.08 ± 0.03°
• Cell volume: 4446.6 ± 1.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1038
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for significantly intense reflections: 0.1145
• Weighted residual factors for all reflections included in the refinement: 0.1376
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No