Information card for entry 4500668

Structure parameters

• Formula: H72 K18 Mn9 O156 Si4 W34
• Calculated formula: K6 Mn9 O156 Si4 W34
• Title of publication: Three Transition-Metal Substituted Polyoxotungstates Containing Keggin Fragments: From Trimer to One-Dimensional Chain to Two-Dimensional Sheet
• Authors of publication: Chen, Lijuan; Shi, Dongying; Zhao, Junwei; Wang, Yulong; Ma, Pengtao; Wang, Jingping; Niu, Jingyang
• Journal of publication: Crystal Growth & Design
• Year of publication: 2011
• Journal volume: 11
• Journal issue: 5
• Pages of publication: 1913
• a: 12.722 ± 0.011 Å
• b: 17.742 ± 0.016 Å
• c: 20.62 ± 0.019 Å
• α: 91.844 ± 0.015°
• β: 107.857 ± 0.015°
• γ: 108.924 ± 0.015°
• Cell volume: 4146 ± 6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2012
• Residual factor for significantly intense reflections: 0.1062
• Weighted residual factors for significantly intense reflections: 0.2548
• Weighted residual factors for all reflections included in the refinement: 0.3116
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No