Information card for entry 4504173

Structure parameters

• Formula: H106 K6 Na18 Ni10 O185 Si4 W34
• Calculated formula: K6 Na18 Ni10 O185 Si4 W34
• Title of publication: Synthesis, Characterization, and Crystal Structures of Double-Cubane-Substituted and Asymmetric Penta-Ni-Substituted Dimeric Polyoxometalates
• Authors of publication: Zhang, Zhiming; Wang, Enbo; Qi, Yanfei; Li, Yangguang; Mao, Baodong; Su, Zhongmin
• Journal of publication: Crystal Growth & Design
• Year of publication: 2007
• Journal volume: 7
• Journal issue: 7
• Pages of publication: 1305
• a: 18.435 ± 0.004 Å
• b: 21.92 ± 0.004 Å
• c: 25.095 ± 0.005 Å
• α: 81.44 ± 0.03°
• β: 73.87 ± 0.03°
• γ: 85.31 ± 0.03°
• Cell volume: 9624 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1181
• Residual factor for significantly intense reflections: 0.0675
• Weighted residual factors for significantly intense reflections: 0.1684
• Weighted residual factors for all reflections included in the refinement: 0.2011
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No