Information card for entry 4504858

Structure parameters

• Formula: C12 H48 Mo8 N12 Ni3 O48 P V8
• Calculated formula: C12 H48 Mo8 N12 Ni3 O48 P V8
• Title of publication: 3D Supramolecular Array Assembled by Cross-like Arrangement of 1D Sandwich Mixed Molybdenum−Vanadium Polyoxometalate Bridged Coordination Polymer Chains: Hydrothermal Synthesis and Crystal Structure of {[MoVI5MoV3VIV8O40(PO4)][Ni(en)2]}[Ni(en)2]2·4H2O
• Authors of publication: Liu, Cai-Ming; Zhang, De-Qing; Zhu, Dao-Ben
• Journal of publication: Crystal Growth & Design
• Year of publication: 2005
• Journal volume: 5
• Journal issue: 4
• Pages of publication: 1639
• a: 26.186 ± 0.005 Å
• b: 13.52 ± 0.003 Å
• c: 19.559 ± 0.004 Å
• α: 90°
• β: 106.6 ± 0.03°
• γ: 90°
• Cell volume: 6636 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.0948
• Weighted residual factors for all reflections included in the refinement: 0.0987
• Goodness-of-fit parameter for all reflections included in the refinement: 0.932
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No