The Phenomenon of Conglomerate Crystallization. Part 57. Control of the Crystallization Behavior by the Choice of the Counter Ion. Part 9. The Stereochemistry and Crystallization Architecture of [(3,2,3-tet)Co(N3)2]X (X = Cl(I), Br(II), I(III), NO3(IV), and PF6(V))
Authors of publication
Saha, Manas K.; Ramanujam, Rathnakumar; Bernal, Ivan; Fronczek, Frank R.
Journal of publication
Crystal Growth & Design
Year of publication
2002
Journal volume
2
Journal issue
3
Pages of publication
205
a
9.9239 ± 0.0003 Å
b
10.0786 ± 0.0003 Å
c
15.1643 ± 0.0005 Å
α
90°
β
92.782 ± 0.001°
γ
90°
Cell volume
1514.93 ± 0.08 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0645
Residual factor for significantly intense reflections
0.0367
Weighted residual factors for significantly intense reflections
0.0721
Weighted residual factors for all reflections included in the refinement
0.0805
Goodness-of-fit parameter for all reflections included in the refinement
