Information card for entry 4506015
| Formula |
C24 H19 Mn N4 O5.5 |
| Calculated formula |
C24 H16 Mn N4 O5.5 |
| Title of publication |
Temperature-Dependent in Situ Reduction of 4,4′-Azobispyridine via Solvothermal Reaction |
| Authors of publication |
Gai, Yan-Li; Jiang, Fei-Long; Xiong, Ke-Cai; Chen, Lian; Yuan, Da-Qiang; Zhang, Lin-Jie; Zhou, Kang; Hong, Mao-Chun |
| Journal of publication |
Crystal Growth & Design |
| Year of publication |
2012 |
| Journal volume |
12 |
| Journal issue |
4 |
| Pages of publication |
2079 |
| a |
16.185 ± 0.007 Å |
| b |
13.588 ± 0.005 Å |
| c |
11.01 ± 0.004 Å |
| α |
90° |
| β |
110.91 ± 0.006° |
| γ |
90° |
| Cell volume |
2261.9 ± 1.5 Å3 |
| Cell temperature |
113 ± 2 K |
| Ambient diffraction temperature |
293 ± 2 K |
| Number of distinct elements |
5 |
| Space group number |
5 |
| Hermann-Mauguin space group symbol |
C 1 2 1 |
| Hall space group symbol |
C 2y |
| Residual factor for all reflections |
0.0557 |
| Residual factor for significantly intense reflections |
0.042 |
| Weighted residual factors for significantly intense reflections |
0.0886 |
| Weighted residual factors for all reflections included in the refinement |
0.0953 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.016 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/4506015.html
